• JAD 191 Allied Chemist NBC 24 Sept 2010


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    • Abstract: MPOB p2.13 (2004) AOCS Cc 10a-25 (1993) AOCS Cc 12-59 (1993) MS 817 ... MPOB Test Methods, A Compendium of Test on Palm Oil and Palm Oil Products, Palm ...

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Issue Date: 24 September 2010
Valid until: 7 July 2012
NO: SAMM 191
(Issue 2, 24 September 2010 replacement of SAMM 191 dated 13 July 2009)
Page 1 of 9
LABORATORY LOCATION : ALLIED CHEMISTS LABORATORY SDN. BHD.
(PERMANENT LABORATORY) 10, JALAN BAKAWALI 68,
TAMAN JOHOR JAYA,
81100 JOHOR BAHRU.
The standard used for assessment of this laboratory is MS ISO/IEC 17025:2005
FIELD OF TESTING : CHEMICAL
SCOPE OF ACCREDITATION :
Materials / Type of tests / Standard test
Products Properties measured / methods /
tested Range of measurement Equipment / Techniques
Water and Effluents Alkalinity APHA 2320 B
(Potable water
Industrial water Calcium APHA 3500-Ca D
Waste water/ Effluents)
Chemical Oxygen Demand APHA 5220 B
Chloride APHA 4500-C1 B
Hardness APHA 2340 C
Iron APHA 3500-Fe D
Magnesium APHA 3500-Mg E
Nitrogen (Ammonia) APHA 4500-NH3 B
APHA 4500-NH3 C
Oil & Grease APHA 5520 B
pH Value APHA 4500-H B
Sulphate APHA 4500-S04 E
Total Suspended Solids APHA 2540 D
Total Solids APHA 2540 B
Preliminary Treatment of Samples for APHA 3030 E
Metal Analysis APHA 3030 F
APHA 3030 G
Issue Date: 24 September 2010
Valid until: 7 July 2012
NO: SAMM 191
(Issue 2, 24 September 2010 replacement of SAMM 191 dated 13 July 2009)
Page 2 of 9
FIELD OF TESTING : CHEMICAL
SCOPE OF ACCREDITATION :
Materials / Type of tests / Standard test
Products Properties measured / Methods /
Tested Range of measurement Equipment / Techniques
Water and Effluents
(continued) Calcium APHA 3500-Ca B/ APHA 3111 B
Copper APHA 3500-Cu B/ APHA 3111 B
Iron APHA 3500-Fe B/ APHA 3111 B
Lead APHA 3500-Pb B/ APHA 3111 B
Magnesium APHA 3500-Mg B/ APHA 3111 B
Manganese APHA 3500-Mn B/ APHA 3111 B
Nickel APHA 3500-Ni B/ APHA 3111 B
Sodium APHA 3500-Na B/ APHA 3111 B
Zinc APHA 3500-Zn B/ APHA 3111 B
Biochemical Oxygen Demand APHA 5210 B/ APHA 4500-O C
(BOD5 at 20° C)
Rubber & Palm Oil Chemical Oxygen Demand (COD) DOE Malaysia Standard Methods
nd
Effluents 2 Ed (1985) Reference Method
Total Nitrogen DOE Malaysia Standard Methods
nd
2 Ed (1985) Reference Method
Ammoniacal Nitrogen DOE Malaysia Standard Methods
nd
2 Ed (1985) Reference Method
Suspended Solids DOE Malaysia Standard Methods
nd
2 Ed (1985) Reference Method
Oil & Grease DOE Malaysia Standard Methods
nd
2 Ed (1985) Reference Method for
treated effluent
Issue Date: 24 September 2010
Valid until: 7 July 2012
NO: SAMM 191
(Issue 2, 24 September 2010 replacement of SAMM 191 dated 13 July 2009)
Page 3 of 9
FIELD OF TESTING : CHEMICAL
SCOPE OF ACCREDITATION:
Materials / Type of tests / Standard test
Products Properties measured / Methods /
Tested Range of measurement Equipment / Techniques
Food & Feeds Total Nitrogen MS 1120 (1988)
(Animal feeds & Feedstuff
Sauces) Nitrogen / Crude Protein MS ISO 5983 (1996)
Phosphorus MS ISO 6491 (1996)
Water-Soluble Chloride MS ISO 6495 (1996)
Moisture in animal feed AOAC 930.15
Ash of flour AOAC 923.03
Protein, Total in flour AOAC 920.87
Crude Fat AOAC 945.18A, AOAC 920.39
MS 1416 (1997)
Total Carbohydrate AOAC : Methods of Analysis for
(by calculation) Nutritional labeling (1993) : page 8
Calories ( by calculation) AOAC : Methods of Analysis for
Nutritional Labelling (1993) : page 5
Oils and Fats Acidity /Acid Value /F.F.A. AOCS Ca 5a-40 (1993)
(Palm Oils & its related MS 817 (1989)
Products Edible Oils) MPOB p2.5 (2004)
Apparent Density MS 817 (1989)
MPOB p4.5 (2004)
Cloud Point AOCS Cc 6-25 (1993)
MS 817 (1989)
MPOB p4.3 (2004)
Cold Test AOCS Cc 11-53 (1993)
Colour (Lovibond) AOCS Cc 13e-92 (1993)
MS 817 (1989)
MPOB p4.1 (2004)
Issue Date: 24 September 2010
Valid until: 7 July 2012
NO: SAMM 191
(Issue 2, 24 September 2010 replacement of SAMM 191 dated 13 July 2009)
Page 4 of 9
FIELD OF TESTING : CHEMICAL
SCOPE OF ACCREDITATION :
Materials / Type of tests / Standard test
Products Properties measured / Methods /
Tested Range of measurement Equipment / Techniques
Oils and Fats DOBI (Deterioration of MS 817 (1989)
(Palm Oils & its related Bleachability Index) MPOB p2.9 (2004)
Products Edible Oils)
Continued Insoluble Impurities AOCS Ca 3a-46 (1993)
MS 817 (1989)
MPOB p2.2 (2004)
Iodine Value AOCS Cd ld-92 (1990)
MPOB p3.2 (2004)
Moisture & Volatile Matter AOCS Ca 2b-38 (1993)
(Hot Plate)
Peroxide Value AOCS Cd 8-53 (1993)
MS 817 (1989)
MPOB p2.3 (2004)
Phosphorus MS 817 (1989)
MPOB p2.8 Part 1(b) (2004)
Saponification Value MS 817 (1989)
MPOB p3.1 (2004)
Slip Melting Point AOCS Cc 3-25 (1993)
MS 817 (1989)
MPOB p4.2 (2004)
Soap Content AOCS Cc 17-79 (1993)
MS 817 (1989)
MPOB p2.13 (2004)
Specific Gravity AOCS Cc 10a-25 (1993)
Titre AOCS Cc 12-59 (1993)
MS 817 (1989)
MPOB p4.6 (2004)
Issue Date: 24 September 2010
Valid until: 7 July 2012
NO: SAMM 191
(Issue 2, 24 September 2010 replacement of SAMM 191 dated 13 July 2009)
Page 5 of 9
FIELD OF TESTING : CHEMICAL
SCOPE OF ACCREDITATION :
Materials / Type of tests / Standard test
Products Properties measured / Methods /
tested Range of measurement Equipment / Techniques
Oils and Fats
(Palm oils & its related Unsaponifiable Matter AOCS Ca 6a-40 (1993)
products, Edible oils) MS 817 (1989)
-Continue MPOB p2.7 Part 2 (2004)
Volatile Matter MS 817 (1989)
MPOB p2.1 Part 1 (2004)
Mineral Oil (Qualitative) AOAC 945.102 (1995)
Mineral Acidity BS 684:2.10 (1988)
Oils and Fats Fat In-house method LWI-MOF 022
(Margarine/Butter) based on Pearson’s Composition
and Analysis of Food, 9th Edition
Salt Content In-house method LWI-MOF 021
based on Pearson’s Composition
th
and Analysis of Food, 9 Edition
Glycerine Identification (Qualitative) British Pharmacopoeia 2001,
Method C
Residue on Ignition
rd
US Pharmacopoeia 23 Edition pg
Fatty acid and Ester 611
rd
US Pharmacopoeia 23 Edition pg
611
Ambient Air Total suspended particulate in ambient ISC Method 501
air.
Nitrogen dioxide in ambient air. ISC Method 406
Sulfur dioxide in ambient air. ISC Method 704C & APHA 4500-
SO4 E
Issue Date: 24 September 2010
Valid until: 7 July 2012
NO: SAMM 191
(Issue 2, 24 September 2010 replacement of SAMM 191 dated 13 July 2009)
Page 6 of 9
FIELD OF TESTING : CHEMICAL
SCOPE OF ACCREDITATION :
Materials / Type of tests / Standard test
Products Properties measured / Methods /
tested Range of measurement Equipment / Techniques
Chimney emission Determination of dark smoke emissions from US Bureau of Mines, IC8333,
chimney using Ringelmann smoke chart. 1967
Determination of sampling and velocity traverse USEPA Method 1
points for chimney.
Determination of chimney gas velocity & USEPA Method 2
volumetric flow rate (Type S pitot).
Determination of chimney gas dry molecular USEPA Method 3
weight.
Determination of moisture content in chimney USEPA Method 4
gases.
Determination of particulate matter emissions USEPA Method 5
from chimney – Isokinetic Method.
Determination of sulfuric acid mist (including USEPA Method 8
sulfur trioxide) emissions from chimney –
Isokinetic Method.
Sampling of polychlorinated dibenzo-p-dioxins USEPA Method 23
and polychlorinated dibenzofurans emissions
from chimney – Isokinetic Method.
Sampling of hydrochloric acid, hydrofluoric acid USEPA Method 26A
and chlorine emissions from chimney emissions
– Isokinetic Method.
Determination of arsenic, cadmium, chromium, USEPA Method 29
copper, lead, mercury and zinc emissions from
chimney – Isokinetic Method.
Measurement of oxygen, carbon dioxide, carbon In-house method WI-EQ-FGA-
monoxide, nitrogen monoxide, nitrogen oxides 001 based on manufacturer
and sulfur dioxide emissions from chimney. manual – MRU GmbH
Environmental Noise Environmental noise levels measurement ISO 1996/1
Issue Date: 24 September 2010
Valid until: 7 July 2012
NO: SAMM 191
(Issue 2, 24 September 2010 replacement of SAMM 191 dated 13 July 2009)
Page 7 of 9
FIELD OF TESTING : MICROBIOLOGY
SCOPE OF ACCREDITATION :
Materials / Type of tests / Standard test
Products Properties measured / Methods /
tested Range of measurement Equipment / Techniques
Potable & Industrial Heterotrophic Plate Count APHA 9215 B
Water
(Microbiological) Total Coliform Count APHA 9222 B
APHA 9221 D
Legionella spp AS/NZS 3986:1998
Pseudomonas aeruginosa APHA 9213 E
th
Food Products Aerobic Plate Count FDA-BAM, 8 Ed, Chap 3
(Microbiological)
th
Total Coliform Count FDA-BAM, 8 Ed, Chap 4
th
Escherichia coli FDA-BAM, 8 Ed, Chap 4
th
Fecal Coliform FDA-BAM, 8 Ed, Chap 4
th
Salmonella spp. FDA-BAM, 8 Ed, Chap 5
th
Staphylococcus FDA-BAM, 8 Ed, Chap 12
th
Yeast & Mould FDA-BAM, 8 Ed, Chap 18
Vibrio parahaemolyticus Australian Std. Food Microbiology
AS 1766.2.9-1991
Mesaphilic aerobic APHA Compendium of Methods for the
Microbiological Examination of Food
Chapter 22
Bacillus cereus APHA Compendium of Methods for the
Microbiological Examination of Food
Chapter 32
Enterobacter sakazakii US Food and Drugs administration Center
for Food Safety and Applied Nutrition
Reused August 2002
Issue Date: 24 September 2010
Valid until: 7 July 2012
NO: SAMM 191
(Issue 2, 24 September 2010 replacement of SAMM 191 dated 13 July 2009)
Page 8 of 9
FIELD OF TESTING : MICROBIOLOGY
SCOPE OF ACCREDITATION :
Materials / Type of tests / Standard test
Products Properties measured / Methods /
tested Range of measurement Equipment / Techniques
Food Listeria monocytogenes Food Drug Administration
Bacteriological Analytical Manual Chapter 10
Thermophilic Flat Sour Compendium of Methods for the
Sporeformers Microbiological Examination of Foods
Fourth Edition, Chapter 25
Howard Mould Count AOAC 984.29 Chapter 16, 1995
Vibrio parahaemolyticus Food Drug Administration
Bacteriological Analytical Manual Chapter 9
Vibrio cholerae Food Drug Administration
Bacteriological Analytical Manual Chapter 9
Fruit Beverages Aerobic Plate Count Compendium of Methods for the
Microbiological Examination of Foods
Fourth Edition, Chapter 58
Water Total Plate Count APHA 9215 D – Membrane Filter
Total Coliform APHA 9221 B – MPN
Fecal Coliform APHA 9221.E.1 – MPN
E. coli APHA 9221 F – MPN
Issue Date: 24 September 2010
Valid until: 7 July 2012
NO: SAMM 191
(Issue 2, 24 September 2010 replacement of SAMM 191 dated 13 July 2009)
Page 9 of 9
Notes:
AOAC Association of Official Analytical Chemists
AOCS Official Methods of American Oil Chemists’ Society (1993)
BS British Standards
DOE Department of Environment Malaysia, Standard Methods (1985)
th
FDA-BAM USA Food and Drug Administration-Bacteriological Analytical Manual (8 Edition)
MS Malaysian Standards
MPOB MPOB Test Methods, A Compendium of Test on Palm Oil and Palm Oil Products, Palm
Kernel Products, Fatty Acids, Food Related Products and Others (2005)
AOAC Association of Official Analytical Chemists
rd
ISC Intersociety Committee Methods of Air Sampling and Analysis, 3 Edition, 1989.
USEPA United States Environmental Protection Agency.
ISO International Organization of Standardization.
th
APHA Standard Method for the Examination of Water and Wastewater, 19 edition 1995,
American Public Health Association (APHA), American Water Work Association (AWWA)
and Water Environment Federation (WEF).
Signatories:
1. Soh Song Chaw IKM No. A 1782/88 (for all accredited testing)
2. Ng Beng Choo IKM No. A 2366/94 (for all accredited testing)
3. Soh Ee Shan IKM No. A 2814/5223/07/09 (Environmental)
4. Azmahani Abd Razak I/C No. 810211-01-6550 (Microbiology)


Use: 0.0263